Exploring novel synthesis and reactivity of diazo compounds and diazo surrogates: studies in batch and continuous flow

Flow reactions were set up on a Vapourtec® E-series Easy MedChemTM flow system. All necessary reactors and accessories were assembled as shown above. Before starting reactions, all reactor tubing were primed with MeOH. Back pressure was set to 3 bar at 5 mL/min. A solution of the acetylhydrazone I-1d and a second another solution of PIDA (1.1 equiv), both in a 1:1 MeOH:CH2Cl2

• Tanbouza, N

• Québec, Canada

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