Microwave irradiation and flow chemistry for a straightforward synthesis of piano-stool iron complexes

    • Anastassiya Pagnoux-Ozherelyevaa
    • David Bolienb
    • Sylvain Gaillarda
    • Flavie Peudrua
    • Jean-François Lohiera
    • Richard J. Whitbyb
    • Jean-Luc Renauda
    • aNormandie University, University of Caen Basse Normandie, Laboratoire de Chimie Moléculaire et Thioorganique, CNRS, Caen, France
    • bChemistry, University of Southampton, Southampton, UK

    Two series of piano-stool iron(II) complexes bearing bidentate phosphine or mixed phosphorus–nitrogen ligands have been prepared upon reaction with CpFe(CO)2I or [CpFe(naphthalene)][PF6] under microwave irradiation or using flow chemistry.

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