Microwave irradiation and flow chemistry for a straightforward synthesis of piano-stool iron complexes

• Anastassiya Pagnoux-Ozherelyeva^a
• David Bolien^b
• Sylvain Gaillard^a
• Flavie Peudru^a
• Jean-François Lohier^a
• Richard J. Whitby^b
• Jean-Luc Renaud^a

• ^aNormandie University, University of Caen Basse Normandie, Laboratoire de Chimie Moléculaire et Thioorganique, CNRS, Caen, France
• ^bChemistry, University of Southampton, Southampton, UK

Two series of piano-stool iron(II) complexes bearing bidentate phosphine or mixed phosphorus–nitrogen ligands have been prepared upon reaction with CpFe(CO)2I or [CpFe(naphthalene)][PF6] under microwave irradiation or using flow chemistry.

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